Ultrasound-Assisted Emulsification Microextraction Based on Solidification Floating Organic Drop Trace Amounts of Manganese Prior to Graphite Furnace Atomic Absorption Spectrometry Determination
نویسندگان
چکیده
منابع مشابه
Ultrasound-Assisted Emulsification Microextraction Based on Solidification Floating Organic Drop Trace Amounts of Manganese Prior to Graphite Furnace Atomic Absorption Spectrometry Determination
In the present study, an ultrasound-assisted emulsification microextraction based on solidification floating organic drop method is described for preconcentration of trace amounts of Mn (II). 2-(5-Bromo-2-pyridylazo)-5 diethylaminophenol was added to a solution of Mn(+2) at ph = 10.0. After this, 1-undecanol was added to the solution as an extraction solvent, and solution was stirred. Several f...
متن کاملDispersive liquid–liquid microextraction based on solidification of floating organic drop combined with flame atomic absorption spectrometry for determination trace amount of cobalt in water samples
An efficient, rapid, simple, and highly selective dispersive liquid–liquid microextraction basedon solidification of floating organic drop (DLLME-SFOD), combined with flame atomicabsorption spectrometry was developed for preconcentration and determination of trace amountsof cobalt in water samples. In this method, an appropriate mixture of acetone and1-undecanol was injected rapidly into the aq...
متن کاملDevelopment of ultrasound-assisted emulsification microextraction for the determination of trace zinc and copper by flame atomic absorption spectrometry
In this work, we developed a method based on ultrasound-assisted emulsification microextraction (USAEME) for the determination of zinc and copper by flame atomic absorption spectrometry (FAAS). The method is based on the use of the organic solvent carbon tetrachloride (CCl4) as an extraction solvent. In order to obtain a high enrichment factor, the effect of different parameters affecting the c...
متن کاملPreconcentration of acrylamide with dispersive liquid-liquid microextraction based on solidification of floating organic drop prior to determination by HPLC
A novel, rapid, simple and sensitive dispersive liquid-liquid microextraction method based on the solidification of floating organic drop (DLLME-SFO) combined with high performance liquid chromatography-ultra violet detection (HPLC-UV) was used to determine acrylamide in potato chips. The derivation of the acrylamide happened in the presence of KBr, KBrO3, H2SO4. Based on studies, 1-undecanol w...
متن کاملFlame atomic absorption spectrometry determination of trace amounts of nickel ions in water samples after ligandless ultrasound-assisted emulsification microextraction.
In the present work, a new ligandless-ultrasound-assisted emulsification microextraction (LL-USAEME) method was developed for preconcentration trace amounts of nickel as a prior step to its determination by flame atomic absorption spectrometry. Some factors influencing the extraction efficiency of nickel and its subsequent determination were studied and optimized, such as type and volume of the...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: The Scientific World Journal
سال: 2012
ISSN: 1537-744X
DOI: 10.1100/2012/987645